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Supercritical Fluids Accessories
Safety Features
Emergency Pressure Relief Device
In their on-going efforts to make their supercritical fluid and other high pressure systems even safer, Applied Separations Inc. has developed a patent-pending device to relieve the pressure in pressure vessels when the normal inlets and outlets have been clogged after extraction/reaction conditions.
| Pressure relief devices have been in use for years to prevent a catastrophic failure of a pressure vessel. These can take the form of pressure relief valves or rupture discs (A). When the pressure rises to the established limit point (B), the valve opens or the rupture disc fails and the pressure is reduced (C).
The situation shown in Figure 1 is the common response to overpressure conditions.
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| A situation may present itself where an extraction/reaction has been performed causing blockage of the inlet or outlet ports (A). The pressure is not great enough to exceed the relief pressure of the rupture disc, but the contents in the pressure vessel are under pressure (B), an UNSAFE CONDITION. |
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| Often one tries to relieve this unsafe condition, merely by trying to forcibly remove the cap by opening it just a small distance so that the pressure can be bled off. This is usually difficult to do, both in overcoming the pressure and in stopping the forced opening at exactly the right point. The usual result
is that the cap is blown off like a cork on a champagne bottle but with much more dangerous consequences. (Figure 3).
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| Applied Separations Inc. has patented a new device to eliminate the problems associated with this “contents under pressure”, but not over pressure condition. Because of an obstruction on the inside of pressure vessel, the contents are under pressure, (Figure 4). Shown here is the patented relief device that pierces the obstruction layer. |
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| Turning the knob drives the piercing element through a rupture disc and the obstruction layer.(Figure 5), allowing the vessel to depressurize safely. Should the obstruction layer reseal, the process can be repeated continuously until the pressure is released.
The threaded Emergency Pressure Relief Device is simply screwed into one of the unused ports in the vessel cap (top or bottom).
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Applications
We have compiled a comprehensive list of SCF applications available for free. Click here to view the list of the SCF applications you can put to use immediately in your lab.
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